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英文: Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide (27.5%) as oxidant.
中文: 摘要以二乙胺和二硫化碳为原料,经双氧水(27.5%)氧化,一步合成了四乙基秋兰姆化二硫。
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英文: The optimum technical conditions is as follow: ethanol as solvent, n[(C2H5)2NH]:n(CS2):n(H2O2,27.5%)=1.05:1.00:1.00, The reaction was carried out for 1 h at 20~30℃ to give tetraethyl thiuram disulfide in 88.0% yield.
中文: 得出最佳工艺条件为:无水乙醇为溶剂,二乙胺:二硫化碳:双氧水=1.05:1.00:1.00,反应时间1h,反应温度20~30℃,收率达到88.0%。
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