以下为句子列表：
英文: METHODS A Nova-Pak C_8( .9 mm× 00 mm, μm) column and mobile phase of methanol-0.% phosphate dibasic anhydrous(0∶0) were used with a flow rate of 0.7 mL·min~-,detection wavelength was 0 nm,temperature was 0 ℃.
中文: 方法:色谱柱为Nova-Pak C8柱( .9mm× 00mm,μm)柱,以甲醇-0.%磷酸溶液(0∶0)为流动相,流速为0.7mL. m in-,检测波长为 0nm。
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英文: METHODS A phenomenex prodigy ODS column (. mm×0 mm, μm) was used and the mobile phase consisted of methanol-0 mmol·L- sodium l-heptanesulfonate(8: ) ,pH was adjusted to . with glacial acetic acid.
中文: 方法采用Phe- nomenex prodigy ODS 色谱柱(． mm×0 mm,μm),流动相为甲醇-0 mmol·L-庚烷磺酸钠溶液(8: ),冰醋酸调pH至 ．,检测波长 nm,流速 mL·min-。
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英文: METHODS Amodiaquine and hydroxychloroquine(interna standard IS) were analyzed on C_(8) column with a mobile phase of methanol-water-triethylamine-orthophosphoric acid(∶(77.)∶∶(0.),v/v) at the flow rate of(.0) mL·min~(-).
中文: 方法:以羟氯喹为内标,采用C8色谱柱,甲醇-水-三乙胺-磷酸(∶77.∶∶0.,v/v)为流动相,流速:.0mL.
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英文: Method: The Thermo ODS C8 column(0 mm×. mm,μm) was used, the mobile phase was methanol -0.% phosphorie acid solution(8: ) , the flow rate was .0 ml·min- and the detection wavelength was at nm.
中文: 方法:色谱柱为Thermo ODS C8柱(0 mm×． mm,μm),流动相为甲醇-0．％磷酸溶液(8:),流速为．0 ml·min-,检测波长为 nm。 结果:大黄素在0．0-0．9μg(r =0.999 );
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英文: Methods A HPLC method was used with DiamonsilTM C 8(0× . mn, μ m) column and a mobile phase of methanol- 0. % phospho ric acid solution (adjusted the pH to .0 with triethylamine)(0 ∶ 0).
中文: 方法采用HPLC法,流动相:甲醇-0.%磷酸(用三乙胺调pH至.0)(0∶0),色谱柱:DiamonsilTMC8(0×.mn,μm),流速:.0mL/min,柱温: ℃,波长:80nm,进样量:0μL。
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