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METHODS Compound : , dimethyl ( methyl piperazine carbonyl) H pyrrole carboxylic acid ethyl ester;
中文意思:
化合物分别为化合物 : , 二甲基 ( 甲基 甲酰基哌嗪基 ) H 吡咯 甲酸乙酯 ;


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METHODS Compound : , dimethyl ( methyl piperazine carbonyl) H pyrrole carboxylic acid ethyl ester; 化合物分别为化合物 : , 二甲基 ( 甲基 甲酰基哌嗪基 ) H 吡咯 甲酸乙酯 ;
METHODS A Nova-Pak C_8( .9 mm× 00 mm, μm) column and mobile phase of methanol-0.% phosphate dibasic anhydrous(0∶0) were used with a flow rate of 0.7 mL·min~-,detection wavelength was 0 nm,temperature was 0 ℃. 方法:色谱柱为Nova-Pak C8柱( .9mm× 00mm,μm)柱,以甲醇-0.%磷酸溶液(0∶0)为流动相,流速为0.7mL. m in-,检测波长为 0nm。
METHODS A phenomenex prodigy ODS column (. mm×0 mm, μm) was used and the mobile phase consisted of methanol-0 mmol·L- sodium l-heptanesulfonate(8: ) ,pH was adjusted to . with glacial acetic acid. 方法采用Phe- nomenex prodigy ODS 色谱柱(. mm×0 mm,μm),流动相为甲醇-0 mmol·L-庚烷磺酸钠溶液(8: ),冰醋酸调pH至 .,检测波长 nm,流速 mL·min-。
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METHODS HPLC-ELSD was used to determine astragaloside IV in Buzhong Yiqi Wan(concentrated pills). The separation was performed on C_(8) columna with a mixture of acetonitrile-water( 7∶ ) as mobile phase. 方法采用高效液相色谱法蒸发光散射检测器测定,A lltech C8色谱柱um(.×0mm),流动相为乙腈-水( 7∶ );
 
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